Conclusive Growth of CdTe Nanorods by Solvothermal Decomposition Using Single Source Precursors

Tiwari, Arunendera Kumar and Verma, Vinay Kumar and Jain, Tripti A. and Bajpai, Parmendra Kumar (2013) Conclusive Growth of CdTe Nanorods by Solvothermal Decomposition Using Single Source Precursors. Soft Nanoscience Letters, 03 (03). pp. 52-57. ISSN 2160-0600

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Abstract

CdTe nanorods are synthesized by solvothermal decomposition, using single source molecular precursors (SSMP) cadmium (II), complex of bis-(aminopropyl telluride) (SSMP-I) and cadmium (II) bis-(isopropyl telluro) propane (SSMP-II) and quinoline as solvent at relatively low temperature (210°C). As synthesized nanomaterials are structurally characterized by XRD and SEM, SEM micrographs revealed formation of rod shapes structures whose dimensions change with the source precursor molecule. The average crystallite size estimated from XRD data is 29.78 and 28.94 nm respectively using Precursors I and II. The average size of nanorods is 1.237 μm and 0.15μm respectively, estimated from SEM micrographs. These are much larger than the average crystallite size estimated from XRD data. This is attributed to the agglomeration of nanocrystallites as quinoline is not a good capping agent.

Item Type: Article
Subjects: Eprints AP open Archive > Medical Science
Depositing User: Unnamed user with email admin@eprints.apopenarchive.com
Date Deposited: 15 Jul 2023 05:43
Last Modified: 17 Oct 2023 05:47
URI: http://asian.go4sending.com/id/eprint/926

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